KRISS Develops World’s First Coffee Bean CRM for Elemental Analysis

- New CRM enables accurate measurement of nutritional and harmful components in coffee beans -

- Expected to enhance quality control of coffee beans and contribute to related basic studies through international cooperation -

# Coffee is an indispensable beverage in the daily lives of Koreans. In Korea, the per capita coffee consumption of the adult population is 2.7 times higher than the global average, and coffee imports (raw and roasted beans) reached a record high of 200,000 tons, amounting to approximately 1.7 trillion won last year. For food items like coffee, which are closely tied to daily routines, stringent quality control is crucial because they are highly sensitive to the reliability. The key to rigorous food quality management lies in the development of reference materials that assist in accurate component analysis.

The Korea Research Institute of Standards and Science (KRISS, President Dr. Ho Seong Lee) has developed the world’s first CRM(Certified Reference Material) capable of accurate measurement of the nutritional and harmful elements in coffee beans.

▲ The KRISS research team

A CRM, which provides accurate measurement values certified by an authoritative body, serves as a standard providing a reference for verifying the accuracy of measurement results and analysis methods. The newly developed coffee bean CRM allows for the accurate measurement of five nutritional elements (calcium, magnesium, iron, zinc, copper) and three harmful elements (lead, mercury, cadmium) within coffee beans.

According to domestic regulations, the permissible limit for the total lead content in roasted coffee, instant coffee, and other coffee products is 2 mg/kg or less. In Europe, the cadmium content in dried edible coffee beans is regulated to be 0.05 mg/kg or less, and the lead content is restricted to 1 mg/kg or less. The lead, mercury, and cadmium content in this CRM are all approximately 0.1 mg/kg, which meets the standards for both domestic and European regulations.

▲ The coffee bean CRM for elemental analysis

To develop this CRM, the Inorganic Metrology Group at KRISS freeze-dried a large quantity of raw coffee beans and obtained a homogeneous sample through multiple grinding and mixing processes. The sample was then sterilized through irradiation, producing a CRM with outstanding stability and homogeneity.

To provide certified measurement values with the world’s highest level of accuracy, this CRM employs isotope dilution mass spectrometry for measurement, one of the most reliable measurement methods in the field of chemistry. With this method, KRISS achieved an accuracy which is more than three times better than that of the conventional measurement methods used by food testing institutions.

▲ The KRISS research team is measuring elemental components using isotope dilution mass spectrometry.

While coffee is widely favored with a substantial volume of international trade, a CRM for elemental analysis of coffee beans, allowing their quality control, has been absent. The newly developed coffee bean CRM by KRISS, however, is expected not only to enhance the measurement reliability and evaluation system of domestic food testing institutions but also to contribute to various fundamental coffee-related research through international collaboration such as overseas distribution.

Dr. Kyoung Seok Lee, the director of Division of Chemical and Biological Metrology, said, “This achievement represents a technological advancement that can significantly improve the quality control level of coffee, a popular beverage as well as heavily imported product. KRISS will continue to develop CRMs for foods such as Korean cabbage, blueberry, and pork, so as to make healthy and safe dining table for the nation.

The coffee bean CRM, developed with support from the fundamental project of KRISS, is currently available on the KRISS Measurement Service website (eshop.kriss.re.kr).